Module A9 · CSEC Chemistry
Oxidation– Reduction

Electrons on the move — from OIL RIG and half equations to oxidation numbers, test reagents, and real-world redox from rusting to breathalysers.

Section 1 — The Big Picture: What is Redox?

A redox reaction occurs when electrons are transferred between substances. One substance loses electrons (is oxidised) and another gains them (is reduced). They always happen together — you can never have one without the other!

OIL
Oxidation Is Loss
of electrons
Mg → Mg²⁺ + 2e⁻
Oxidation number INCREASES
RIG
Reduction Is Gain
of electrons
Cu²⁺ + 2e⁻ → Cu
Oxidation number DECREASES
💡 Golden Rule Oxidation and reduction ALWAYS occur simultaneously. A substance that loses electrons (oxidised) must transfer them somewhere — the receiving substance is reduced. You cannot have oxidation without reduction in the same reaction!
Oxidising Agent Causes another substance to be oxidised. Takes electrons from the other reactant. Is itself reduced (its oxidation number decreases). Examples: Cl₂, KMnO₄, K₂Cr₂O₇, O₂, H₂O₂.
Reducing Agent Causes another substance to be reduced. Donates electrons to the other reactant. Is itself oxidised (its oxidation number increases). Examples: Zn, Fe, H₂, CO, SO₂, H₂S.
🧠 Memory Trick The oxidising agent is itself reduced. The reducing agent is itself oxidised. They're opposites! Think: "The oxidising agent pays the price by being reduced."

Section 2 — Redox in Your Everyday Life

🦀 Rusting

Iron + oxygen + water → hydrated iron(III) oxide (Fe₂O₃·xH₂O) = rust. Iron is oxidised by oxygen. Salt water accelerates rusting because dissolved ions increase electrical conductivity, speeding up electron transfer.

🍎 Browning of Cut Fruit

Enzymes in fruit cells oxidise phenolic compounds to dark melanins. Lemon juice (Vitamin C / ascorbic acid) acts as a reducing agent — it is oxidised preferentially, slowing the browning of the fruit.

🧴 Bleaches

Chlorine bleaches (NaClO) and oxygen bleaches (H₂O₂) are oxidising agents that remove stains by oxidising coloured dye molecules to their colourless form. The bleach is reduced in the process.

🚗 Breathalyser Test

Acidified potassium dichromate(VI) (K₂Cr₂O₇) tests for alcohol. Ethanol in breath reduces the orange Cr₂O₇²⁻ ion to the green Cr³⁺ ion. Orange → Green = positive test!

🍷 Food Preservation with SO₂ Sodium sulfite (Na₂SO₃) and sulfur dioxide (SO₂) are used as food preservatives in wine, dried fruit, and juices. They act as reducing agents — they are oxidised preferentially, preventing the oxidation (spoilage/discolouration) of the food itself.

Section 3 — Half Equations

Any redox reaction can be split into two half equations — one showing oxidation, one showing reduction. Each half equation must balance in both atoms AND charge.

Worked Example — Zn + CuSO₄

Oxidation Half (Zn loses electrons)

Zn(s) → Zn²⁺(aq) + 2e⁻

Zn starts at 0, ends at +2 → oxidation number INCREASES → oxidised. Zn is the reducing agent.

Reduction Half (Cu²⁺ gains electrons)

Cu²⁺(aq) + 2e⁻ → Cu(s)

Cu starts at +2, ends at 0 → oxidation number DECREASES → reduced. Cu²⁺ is the oxidising agent.

Adding the half equations (electrons cancel):

Zn(s) + Cu²⁺(aq) → Zn²⁺(aq) + Cu(s) Or with full ionic: Zn(s) + CuSO₄(aq) → ZnSO₄(aq) + Cu(s) ✓ Atoms balance ✓ Charges balance ✓ Electrons cancel

Worked Example — Breathalyser (Acidified K₂Cr₂O₇)

Oxidation Half (Ethanol oxidised)

C₂H₅OH → CH₃COOH + 4H⁺ + 4e⁻

Ethanol (C=−1 average) → Ethanoic acid (C=0 average). Ethanol is oxidised. It is the reducing agent.

Reduction Half (Dichromate reduced)

Cr₂O₇²⁻ + 14H⁺ + 6e⁻ → 2Cr³⁺ + 7H₂O

Cr: +6 → +3 (decrease) → reduced. K₂Cr₂O₇ is the oxidising agent. Orange → Green colour change.

💡 Exam Tip — Checking Half Equations Always verify: (1) Atoms balance on both sides. (2) Charges balance — sum of charges on left = sum on right. (3) Include state symbols (s), (l), (g), (aq). If you need to balance oxygen, add H₂O. If you need to balance hydrogen, add H⁺ (in acid conditions).

Section 4 — Oxidation Numbers

An oxidation number (oxidation state) is the theoretical charge an atom would have if all its bonds were ionic. It lets us track electron transfer and identify what has been oxidised or reduced.

Rules for Assigning Oxidation Numbers

Rule 1Free element: Oxidation number = 0. Examples: Na, O₂, Cl₂, Fe — all are zero.
Rule 2Monatomic ion: Oxidation number = ion charge. Mg²⁺ → +2, Cl⁻ → −1, Fe³⁺ → +3.
Rule 3Hydrogen in compound: Usually +1. Exception: metal hydrides (NaH, CaH₂) → H is −1.
Rule 4Oxygen in compound: Usually −2. Exception: peroxides (H₂O₂, Na₂O₂) → O is −1.
Rule 5Neutral compound: All oxidation numbers must sum to zero.
Rule 6Polyatomic ion: All oxidation numbers must sum to the ion's charge.

Worked Examples

Example 1: Oxidation number of S in SO₂ Let S = x. x + 2(−2) = 0 → x = +4 SO₂ = sulfur(IV) oxide ✅ Example 2: Oxidation number of N in NO₃⁻ Let N = x. x + 3(−2) = −1 → x = +5 NO₃⁻ = nitrate(V) ion ✅ Example 3: Oxidation number of Cr in K₂Cr₂O₇ 2(+1) + 2(Cr) + 7(−2) = 0 2 + 2Cr − 14 = 0 → Cr = +6 K₂Cr₂O₇ = potassium dichromate(VI) ✅ Example 4: Oxidation number of Mn in KMnO₄ (+1) + Mn + 4(−2) = 0 → Mn = +7 KMnO₄ = potassium manganate(VII) ✅
🧠 Using Oxidation Numbers to Identify Redox In a redox reaction: an atom whose oxidation number increases has been oxidised. An atom whose oxidation number decreases has been reduced. If no oxidation numbers change, it is NOT a redox reaction.

Section 5 — Testing for Oxidising & Reducing Agents

These colour changes must be memorised — they come up constantly in CSEC exams!

Tests for an OXIDISING AGENT

Reagent: KI(aq) (potassium iodide)

Colourless Brown

I⁻ ions are oxidised to I₂ (brown). The unknown oxidising agent takes electrons from I⁻.

Reagent: FeSO₄(aq) (iron(II) sulfate)

Pale green Yellow-brown

Fe²⁺ oxidised to Fe³⁺ by the unknown oxidising agent.

Tests for a REDUCING AGENT

Reagent: Acidified KMnO₄

Purple Colourless

MnO₄⁻ (Mn: +7) reduced to Mn²⁺ (Mn: +2) by the unknown reducing agent. Purple disappears.

Reagent: Acidified K₂Cr₂O₇

Orange Green

Cr₂O₇²⁻ (Cr: +6) reduced to Cr³⁺ (Cr: +3) by the unknown reducing agent.

ReagentTests ForColour ChangeWhat Happens
Potassium iodide KI(aq)Oxidising agentColourless → BrownI⁻ oxidised to I₂
Iron(II) sulfate FeSO₄(aq)Oxidising agentPale green → Yellow-brownFe²⁺ oxidised to Fe³⁺
Acidified KMnO₄ (purple)Reducing agentPurple → ColourlessMnO₄⁻ (+7) reduced to Mn²⁺ (+2)
Acidified K₂Cr₂O₇ (orange)Reducing agentOrange → GreenCr₂O₇²⁻ (+6) reduced to Cr³⁺ (+3)

Section 6 — Substances That Act as Both

Some substances can be oxidising agents OR reducing agents depending on their reaction partner. The key is comparing relative strengths.

Sulfur Dioxide (SO₂)

Usually a REDUCING AGENT (S is at +4, can go up to +6):

SO₂ + Cl₂ + 2H₂O → H₂SO₄ + 2HCl (SO₂ reduces Cl₂; Cl: 0 → −1)

Acts as OXIDISING AGENT with H₂S (stronger reducer):

2H₂S + SO₂ → 3S + 2H₂O (H₂S oxidised; S: −2 → 0)

Hydrogen Peroxide (H₂O₂)

Usually an OXIDISING AGENT:

H₂O₂ + 2KI → I₂ + 2KOH Colourless → Brown (I⁻ oxidised to I₂)

Acts as REDUCING AGENT with stronger oxidisers:

H₂O₂ + acidified KMnO₄ → Purple disappears (H₂O₂ reduces MnO₄⁻)

Section 7 — Resources & Simulations

Section 8 — CSEC Practice Questions

Question 1 — Definitions
Define oxidation and reduction in terms of: (a) electrons, (b) oxidation numbers. State the full name of the memory aid used to recall these definitions.
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a In terms of electrons: Oxidation = loss of electrons. Reduction = gain of electrons.

b In terms of oxidation numbers: Oxidation = increase in oxidation number. Reduction = decrease in oxidation number.

✅ Memory aid: OIL RIG — Oxidation Is Loss, Reduction Is Gain (of electrons).
Question 2 — Identify Redox
In the reaction: Fe₂O₃(s) + 3CO(g) → 2Fe(s) + 3CO₂(g), identify which substance has been oxidised and which has been reduced. Give reasons using oxidation numbers, and state the oxidising and reducing agents.
+

1 Find oxidation number of Fe: In Fe₂O₃, Fe = +3. In Fe(s), Fe = 0. Fe: +3 → 0 (decrease) → REDUCED. Fe₂O₃ is the oxidising agent.

2 Find oxidation number of C: In CO, C = +2. In CO₂, C = +4. C: +2 → +4 (increase) → OXIDISED. CO is the reducing agent.

✅ Fe₂O₃ is reduced (Fe: +3→0), it is the oxidising agent. CO is oxidised (C: +2→+4), it is the reducing agent.
Question 3 — Oxidation Numbers
Calculate the oxidation number of: (a) S in H₂SO₄, (b) N in NH₃, (c) Cl in ClO₄⁻ (perchlorate ion), (d) Mn in MnO₄⁻.
+

a H₂SO₄: 2(+1) + S + 4(−2) = 0 → 2 + S − 8 = 0 → S = +6

b NH₃: N + 3(+1) = 0 → N = −3

c ClO₄⁻: Cl + 4(−2) = −1 → Cl − 8 = −1 → Cl = +7 (perchlorate = chlorate(VII))

d MnO₄⁻: Mn + 4(−2) = −1 → Mn − 8 = −1 → Mn = +7 (manganate(VII) ion)

✅ (a) +6 (b) −3 (c) +7 (d) +7
Question 4 — Test Reagents
A solution turns acidified KMnO₄ from purple to colourless. (a) What type of substance is present? (b) Write the half-equation for KMnO₄ being reduced in acid conditions. (c) Name ONE other reagent that could confirm this result.
+

a KMnO₄ is decolourised → it has been reduced. A reducing agent must be present to donate electrons to the MnO₄⁻ ions.

b Half-equation for reduction of manganate(VII) in acid:

MnO₄⁻(aq) + 8H⁺(aq) + 5e⁻ → Mn²⁺(aq) + 4H₂O(l)

Check: Mn changes from +7 to +2 ✓ (decrease = reduction ✓)

c Acidified K₂Cr₂O₇ — if the solution changes from orange to green, it confirms a reducing agent is present.

✅ (a) A reducing agent. (b) MnO₄⁻ + 8H⁺ + 5e⁻ → Mn²⁺ + 4H₂O. (c) Acidified K₂Cr₂O₇ (orange → green).
Question 5 — Half Equations
Write the half equations for: (a) the oxidation of Fe²⁺ to Fe³⁺, (b) the reduction of Cl₂ to Cl⁻, (c) hence write the overall ionic equation for the reaction between Fe²⁺ and Cl₂.
+

a Fe²⁺ loses 1 electron to form Fe³⁺ (oxidation number +2 → +3, increase = oxidised):

Fe²⁺(aq) → Fe³⁺(aq) + e⁻

b Each Cl atom in Cl₂ gains 1 electron (+0 → −1, decrease = reduced):

Cl₂(g) + 2e⁻ → 2Cl⁻(aq)

c Multiply (a) by 2 so electrons cancel: 2Fe²⁺ → 2Fe³⁺ + 2e⁻, then add to (b):

2Fe²⁺(aq) + Cl₂(g) → 2Fe³⁺(aq) + 2Cl⁻(aq)

✅ 2Fe²⁺(aq) + Cl₂(g) → 2Fe³⁺(aq) + 2Cl⁻(aq). Cl₂ is the oxidising agent; Fe²⁺ is the reducing agent.